National Committee for Quality Assurance

Development and validation of a novel stability indicating RP-UPLC method for the estimation of Leniolisib and characterization of its degradation products by UPLC-MS/MS

Current analytical methods available for the quantification of Leniolisib were predominantly based on conventional HPLC and LC–MS/MS techniques, with each having inherent methodological limitations in terms of longer analysis times, laboratory efficiency and low-throughput indust...

Beyond Execution

Generative artificial intelligence is commonly framed as a challenge to employment, authorship, academic integrity, professional competence and human intellectual distinctiveness. This paper argues that these apparently separate disputes share a deeper institutional problem. For...

Beyond Execution

Generative artificial intelligence is commonly framed as a challenge to employment, authorship, academic integrity, professional competence and human intellectual distinctiveness. This paper argues that these apparently separate disputes share a deeper institutional problem. For...

Impact of Structured Data Validation on Case Completeness and Key Quality Indicators in the SWISS Implant Registry (SIRIS Spine): A SINGLE-CENTER Audit

Study design Retrospective single-center registry validation audit. Objective To quantify the impact of semi-automated, chart-adjudicated data validation workflow on case completeness and key quality indicators in the Swiss Implant Registry (SIRIS Spine). Methods All Swiss proced...

QbD BASED UV AND RP-HPLC METHOD DEVELOPMENT AND VALIDATION OF VILDAGLIPTIN IN BULK API

Abstract The present study aimed to develop and validate UV-Visible spectrophotometric and QbD-based RP-HPLC analytical methods for the quantitative estimation of Vildagliptin in bulk drug. UV spectrophotometric analysis was performed using Methanol:Water (60:40 v/v) as solventan...